Sure thing, here’s a quick, no‑frills protocol that keeps the line of safety clear but still leaves room for surprises. 1. Gather the reagents in a well‑ventilated fume hood, check labels, and make sure all personal protective equipment is on. 2. Measure the limiting reactant with a calibrated pipette; the excess will be your variable. 3. Add the first reactant to the reaction vessel, then swirl gently to ensure full dissolution. 4. Slowly introduce the second reactant while maintaining a steady temperature—use a thermostatted bath set to the optimum point from your literature review. 5. Stir continuously at a moderate speed (about 300 rpm) to avoid local overheating, but let the mixture rest for 10 minutes to allow the first wave of reaction to complete. 6. At the 10‑minute mark, add a controlled amount of catalyst or a shock reagent (e.g., a small aliquot of a strong oxidant) to trigger the next phase. Keep it “just enough” – you want a burst, not a blowout. 7. Monitor the reaction color, pressure, and temperature in real time. If you notice an unexpected exotherm, immediately dilute with ice‑cold solvent or add a neutralizing agent. 8. Once the color change stabilizes, quench the reaction with a stoichiometric amount of a benign scavenger (e.g., a dilute NaOH solution for acidic by‑products). 9. Extract the product with an appropriate organic solvent, dry over anhydrous MgSO₄, and concentrate under reduced pressure. 10. Finally, analyze the crude mixture by TLC or GC‑MS. If the spot pattern looks intriguing, set the sample aside for a scale‑up; if it looks dull, tweak the catalyst load or the temperature for the next run. Remember: keep the safety window tight—no abrupt pressure spikes, no uncontrolled heat—and let the chemistry do its own drama within those boundaries. Happy hunting!